Synthesis and X-ray analysis of 1-((1S)-phenylethyl)-azetidine-(2R)-piperidinamide Version 4.0

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Synthesis and X-ray analysis of 1-((1S)-phenylethyl)-azetidine-(2R)-piperidinamide
deGelder R, Smits JMM, Starmans WAJ, Thijs L, Zwanenburg B
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY 26: (9) 639-642 SEP 1996

Document type: Article

Language: English

Cited References: 13

Times Cited: 2

Abstract:
The crystal and molecular structure of a new azetidine-2-carboxylic amide derivative is described. The structure was solved by direct methods and refined by least squares methods to R1 = 0.0393 for 4264 reflections (with I > 2 sigma(I)). The structure consists of two independent molecules which are chemically the same with slight differences in geometry. Crystal data: C17H24N2O, monoclinic, space group P2(1), a = 8.3782(4), b = 20.0342(13), c = 9.7769(8)Angstrom, beta = 109.687(6)degrees, V = 1545.1(2)Angstrom(3), Z = 4.

Author Keywords:
crystal structure, chiral auxiliaries

Addresses:
deGelder R, CATHOLIC UNIV NIJMEGEN, NIJMEGEN SON RES CTR, DEPT INORGAN CHEM, TOERNOOIVELD, NL-6525 ED NIJMEGEN, NETHERLANDS.
CATHOLIC UNIV NIJMEGEN, NIJMEGEN SON RES CTR, DEPT ORGAN CHEM, NL-6525 ED NIJMEGEN, NETHERLANDS.

Publisher:
PLENUM PUBL CORP, NEW YORK

IDS Number:
VX842

ISSN:
1074-1542

Article 27 of 38